Hyphenated Separation Techniques
Informacje ogólne
Kod przedmiotu: | 0600-S2-EN-HST |
Kod Erasmus / ISCED: |
13.3
|
Nazwa przedmiotu: | Hyphenated Separation Techniques |
Jednostka: | Wydział Chemii |
Grupy: |
studia stacjonarne II stopnia, Chemistry of Advanced Materials semestr 4 |
Punkty ECTS i inne: |
6.00
|
Język prowadzenia: | polski |
Wymagania wstępne: | (tylko po angielsku) General issues of advanced chromatographic and electromigration techniques |
Całkowity nakład pracy studenta: | (tylko po angielsku) Lecture: Total student workload Contact hours with teacher: np. - participation in lectures - 30 hrs - consultations - 15 hrs Self-study hours: np. - preparation for lectures - 15 hrs - writing essays/ papers/ projects - 5 hrs - reading literature - 5 hrs - preparation for test/ examination - 30 hrs Altogether: 100 hrs (7 ECTS) Laboratory: Contact hours with teacher: np. - participation in lectures - 30 hrs - consultations - 15 hrs Self-study hours: np. - preparation for lectures - 15 hrs - writing essays/ papers/ projects - 5 hrs - reading literature - 5 hrs - preparation for test/ examination - 30 hrs Altogether: 100 hrs (7 ECTS) |
Efekty uczenia się - wiedza: | (tylko po angielsku) Lecture: W01: uses and explains terminology specific to the subject in English and its equivalent in Polish - K_W01 W02: recognizes and distinguishes between issues related to the subject of classes - K_W13, K_W14 Laboratory: W01: uses and explains terminology specific to the subject in English and its equivalent in Polish - K_W01 W02: recognizes and distinguishes between issues related to the subject of classes - K_W13, K_W14 |
Efekty uczenia się - umiejętności: | (tylko po angielsku) Lecture: U01: apply theoretical knowledge in practice, including the use of facilities and other small laboratory equipment in a correct and proper way - K_U11. U02: make measurements - K_U11. U03: prepare on their own preparations for the tests, analytical procedures - K_U14. U04: can analyzes, interprets and calculates the results obtained in the laboratory, in the course of his work - K_U11. U05: can develop analytical methodology - K_U14 Laboratory: U01: apply theoretical knowledge in practice, including the use of facilities and other small laboratory equipment in a correct and proper way - K_U11. U02: make measurements - K_U11. U03: prepare on their own preparations for the tests, analytical procedures - K_U14. U04: can analyzes, interprets and calculates the results obtained in the laboratory, in the course of his work - K_U11. U05: can develop analytical methodology - K_U14 |
Efekty uczenia się - kompetencje społeczne: | (tylko po angielsku) Lecture: K01: apply appropriate analytical procedures - K_K02. K02: draw up test reports and notes, which can be used as a basis for the preparation of scientific publications - K_K05. Laboratory: Learning outcomes - social competencies K01: apply appropriate analytical procedures - K_K02. K02: draw up test reports and notes, which can be used as a basis for the preparation of scientific publications - K_K05. |
Metody dydaktyczne: | (tylko po angielsku) Expository teaching methods: - informative lecture - lectures with discussion Laboratory experiments |
Skrócony opis: |
(tylko po angielsku) The aim of course is to familiarize students with the theoretical basics and possibilities of the application of modern methods, especially chromatographic techniques in analytics. |
Pełny opis: |
(tylko po angielsku) Sample preparation using solid phase extraction (SPE) and quantitative analysis by high performance liquid chromatography (HPLC). Application of GC/MS coupled technique. Separation of nanoparticles by field-flow fractionation - FFF. Determination of inorganic ions by ion chromatography. The determination of volatile organic compounds (VOCs) by use of SPME-GC, P&T-GC and LLE-GC methods. The comparison of HPLC and UHPLC techniques. Miniaturized separation techniques: capillary liquid chromatography (nanoLC) and capillary electrophoresis. |
Literatura: |
(tylko po angielsku) 1. B. Buszewski, E. Dziubakiewicz, M. Szumski [red.], Electromigration techniques, Springer-Verlag, Berlin Heidelberg 2013. 2. J.R. Dean, Methods for environmental trace analysis, John Wiley & Sosns Inc., Chichester 2003. 3. B. Ardrey, Liquid chromatography-mass spectrometry: an introduction, John Wiley & Sosns Inc., Chichester 2003. 4. I. Baranowska [Ed.], Handbook of Trace Analysis Fundamentals and Applications, Springer International Publishing 2015. 5. P. Bocek, Analytical capillary isotachophoresis, Verlag Chemie, Weinheim 1987. 6. S. Mitra, Sample preparation techniques in analytical chemistry, Wiley, New Jersey 2003. 7. R.P. W. Scott , Tandem techniques, J. Wiley & Sons, New York 1998. 8. C.F. Poole, The Essence of Chromatography, Elsevier, Amsterdam 2003. 9. J. Pawliszyn [Ed.], Sampling and sample preparation for field and laboratory Elsevier Science B.V., Amsterdam 2002 10. C. F. Poole, S. K. Poole, Chromatography Today, Elsevier, Amsterdam 1991. 11. J. Pawliszyn, Solid Phase Microextraction, Wiley & Sons, New York 1997. 12. D. C. Harris, Quantitative & Qualitative Chemical Analysis, Freeman, New York 1999. |
Metody i kryteria oceniania: |
(tylko po angielsku) To pass of laboratory experiments is the knowledge of analytical procedures required for the correct execution of exercises-laboratory analysis, a positive evaluation of the colloquium preceding the exercise include the written report for each experiment – W01, W02, K02 fail - 2 pts (≥50%) satisfactory - 3 pts (50-60%) satisfactory plus - 3,5 pts (61-65%) good - 4 pts (66-75%) good plus - 4,5 pts (76-80%) very good - 5 pts (≤81%) |
Praktyki zawodowe: |
(tylko po angielsku) Work placement not applicable |
Zajęcia w cyklu "Semestr letni 2023/24" (zakończony)
Okres: | 2024-02-20 - 2024-09-30 |
Przejdź do planu
PN WYK
WT ŚR LAB
CZ PT |
Typ zajęć: |
Laboratorium, 30 godzin
Wykład, 30 godzin
|
|
Koordynatorzy: | Bogusław Buszewski | |
Prowadzący grup: | Szymon Bocian, Sylwia Studzińska | |
Lista studentów: | (nie masz dostępu) | |
Zaliczenie: |
Przedmiot -
Egzamin
Laboratorium - Zaliczenie na ocenę Wykład - Egzamin |
Zajęcia w cyklu "Semestr letni 2024/25" (jeszcze nie rozpoczęty)
Okres: | 2025-02-24 - 2025-09-30 |
Przejdź do planu
PN WT ŚR CZ PT |
Typ zajęć: |
Laboratorium, 30 godzin
Wykład, 30 godzin
|
|
Koordynatorzy: | Bogusław Buszewski | |
Prowadzący grup: | Szymon Bocian, Katarzyna Rafińska | |
Lista studentów: | (nie masz dostępu) | |
Zaliczenie: |
Przedmiot -
Egzamin
Laboratorium - Zaliczenie na ocenę Wykład - Egzamin |
Właścicielem praw autorskich jest Uniwersytet Mikołaja Kopernika w Toruniu.